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1 CONTENTS 2. 2 THERMAL METHODS OF ANALYSIS COURSE 4. 3 THERMODYNAMIC BASES OF THERMOANALYTICAL INVESTIGATIONS 6. 4 THERMOGRAVIMETRY 7. 4.1 INTERPRETATION OF THERMOGRAVIMETRIC CURVES 11. 4.2 FACTORS AFFECTING THE SHAPE OF THERMOGRAVIMETRIC CURVES
Analyzing & Testing. Business Unit www.netzsch.com. Thermal Analysis Methods (Part 1):. TG, DSC, STA, EGA. Practical Applications of Thermal Analysis Methods in Material Science. Krakow, 15 – 16 May, 2012. Ekkehard Post, NETZSCH Geratebau, Wittelsbacher Str. 42, D-95100 Selb/Germany. Krakow 2012/ep
Outline. ? Definitions. ? What is thermal analysis? ? Instrumentation & origin of the TGA-DTA signal. ? TGA. ? DTA. ? Phase diagrams & Thermal analysis. • Thermal analysis,an experimental method to determine phase diagrams. Basics and applications
Consequence. Depending on the engineering design, measuring cell construcion and the way of data representaion, variety of methods has been arisen: DTG, DTA, DSC, STA etc. Andrey Tarasov, Thermal analysis, Lecture series heterogeneous catalysis, FHI MPG, 26.10.12. Basic Principles and Terminology. 6
Thermal Analysis. • TGA can provide information about physical phenomena like vaporization, sublimation, absorption, and desorption. • Also chemical phenomena including dehydration, decomposition and oxidation and reduction reactions.
The method of Differential Thermal Analysis, as it is known, has reached the prominence nf oth«r t.«r>hn1.nn«a fsnch as x-ray diffraction, microscopes, etc. as a helpful research and control tool. Its importance is Increasing because of the develop- ment of equipment refinements, and because of the potential value of the
1.1 Thermal methods and Catalysis. Thermal analysis refers to the variety of techniques developed and used in which any physical property of a given system is continuously measured as a func- tion of temperature, though temperature and time may be related by the term called the heating rate namely dT/dt, this aspect will
Basically, methods of thermal analysis allow the study of all chemical processes that are associated with heating/cooling. And there is a lot of these: decomposition, pyrolysis, ignition, phase changes, calorimetry, etc. All this can be studied on a small amount of sample and in a highly automated way.
22 Dec 2017 Temperature controller: Temperature difference between the sample and reference is measured (Table 3). Table 3: Difference. Aspect. TGA. DTA. DSC. Instrument.
Thermal analysis comprises a group of techniques in which a physical property of a substance is measured as a function of temperature, while the substance is subjected to a controlled temperature programme. In differential thermal analysis, the temperature difference that de- velops between a sample and an inert
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